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Beilstein J. Org. Chem. 2010, 6, No. 26, doi:10.3762/bjoc.6.26
Graphical Abstract
Scheme 1: Bisacylphosphine oxide with improved solubility in polar solvents.
Scheme 2: Etherification of 3-(chloromethyl)-2,4,6-trimethylbenzoic acid and chlorination of 1.
Scheme 3: Rearrangement of 2 under formation of 4.
Scheme 4: Synthesis of WBAPO starting from P,P-dichlorophenylphosphine and 2.
Figure 1: 1H NMR spectra (400 MHz, CDCl3) of BAPO and WBAPO.
Scheme 5: Structure of the main impurity in isolated WBAPO.
Figure 2: UV–vis absorption spectra of WBAPO and CQ dissolved in acetonitrile (10−3 mol/L).
Figure 3: DSC-plot of a mixture of Bis-GMA (42 wt %), UDMA (37 wt %), TEGDMA (21 wt %) and the PI WBAPO or BA...